J4 ›› 2009, Vol. 47 ›› Issue (05): 1065-1070.

• 化学 • 上一篇    下一篇

水相合成磁性Fe3O4纳米颗粒

吴晋瑞1, 薛立娟2, 丁国斌1, 洪霞3, 郭轶1, 黄宜兵1, 徐力1, 张学忠1
   

  1. 1. 吉林大学 分子酶学工程教育部重点实验室, 长春 130021;2. 吉林大学 第一医院, 长春 130021|3. 东北师范大学 物理学院, 长春 130024
  • 收稿日期:2009-01-16 出版日期:2009-09-26 发布日期:2009-11-03
  • 通讯作者: 徐力 E-mail:huangyibing@jlu.edu.cn.

Synthesis of Magnetic Fe3O4 Nanoparticle in Aqueous Phase

WU Jinrui1, XUE Lijuan2, DING Guobin1, HONG Xia3, GUO Yi1,HUANG Yibing1, XU Li1, ZHANG Xuezhong1
   

  1. 1. Key Laboratory for Molecular Enzymology and Engineering of Ministry of Education, Jilin University,Changchun 130021, China|2. First Hospital, |Jilin University, Changchun 130021, China|3. School of Physics, Northeast Normal University, Changchun 130024, China
  • Received:2009-01-16 Online:2009-09-26 Published:2009-11-03
  • Contact: XU Li E-mail:huangyibing@jlu.edu.cn.

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摘要：

采用化学共沉淀法制备Fe3O4纳米粒子, 选择NH3·H2O作为沉淀剂, 并与Fe2+和Fe3+的混合溶液同时同速滴加到由氨水和硝酸氨组成的缓冲溶液中, 制得了磁性Fe3O4纳米粒子. 考察了磁性纳米粒子合成的一些影响因素, 并用透射电镜(TEM)、 X射线粉末衍射(XRD)、 红外光谱等方法对其性质进行了初步表征.

关键词: 化学共沉淀法； 四氧化三铁； 纳米粒子； 磁性

Abstract:

In this work, nanometer magnetite (Fe3O4) particles were prepared by the chemical coprecipitation method, NH3·H2O was chosen as the precipitating agent, and was added dropwise together with the mixed aqueous solution containing ferric and ferrousions to the buffer solution composed of NH3·H2O and ammonium nitrate to produce nanometer Fe3O4 particles. Some influence factors on the size and characteristic of the product were investigated, and preliminary characterization was also performed by means of TEM, XRD and IR spectrum.

Key words: chemical coprecipitation, magnetite, nanometer, magnetism

中图分类号: 

  • O648.1
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