高岭土/肼插层材料的制备与表征

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The Preparation and Characterization of the Kaolin-Hydrazine Intercalation Complex

LI Xian-zhou¹,LIU Yan²,LIU Li-hua¹,NING Wei-kun¹,FAN Hai³

1.College of Material Science & Engineering，Jilin University, Changchun 130025, China；2. Liaoning Science and Technology College, Benxi,Liaoning 117022, China；3. Avigation University of AirForce , Changchun 130022, China

Received:2005-11-06 Revised:1900-01-01 Online:2006-07-26 Published:2006-07-26
Contact: LI Xian-zhou

Abstract

Abstract: With natural mineral kaolinite as raw material, 50% hydration hydrazine as intercalation chemicals, the authors intercalated hydrazine molecules (NH₂-NH₂)between the layers of Kaolinite successfully by direct liquid intercalation,stirring at the same time,and prepared the hydrazine-kaolin intercalation complex material. The product was characterized by the infrared reflectance spectroscopy and the granularity analyse apparatus . The IR spectrum indicate, the new hydrogen bondings was formed in the N-H-OH interaction between the N-H in the hadrazine molecules from intercalation chemicals and the hydroxypyzidone(-OH) in the inner surface of kaolin. The average particle size of the products has increased by 46.84%,and the percent for the particles which radius is less than 5 micron has decreased 10.55%.

Key words: kaolin, intercalation complex, hydrazine

CLC Number:

P619.232

LI Xian-zhou,LIU Yan,LIU Li-hua,NING Wei-kun,FAN Hai. The Preparation and Characterization of the Kaolin-Hydrazine Intercalation Complex[J].J4, 2006, 36(04): 659-662.

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The Preparation and Characterization of the Kaolin-Hydrazine Intercalation Complex

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