三异丙醇胺硼酸酯的合成与表征

Abstract

Abstract:

Triisopropanolamine borate was synthesized through the esterification of triisopropanolamine and boric acid, and purified by recrystallization. The structure of triisopropanolamine borate was characterized by MS, ¹H NMR and FTIR. Effects of raw material ratio, reaction temperature, reaction time, and reaction solvent on the synthesis, and those of recrystallization solvent and solvent ratio on the purification were investigated. The product was obtained with a purity of 99.8% and a yield of 87.1%, respectively.

Key words: triisopropanolamine borate, synthesis, purification

CLC Number:

O627

WANG Wei, XIU Zhiming, WANG Deli, XU Tianshu,GUO Youming, WANG Liping. Synthesis and Characterization of Triisopropanolamine Borate[J].Journal of Jilin University Science Edition, 2014, 52(04): 831-834.

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Synthesis and Characterization of Triisopropanolamine Borate

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