J4 ›› 2013, Vol. 51 ›› Issue (03): 502-504.

• 物理 • 上一篇    下一篇

带状石墨相C3N4化合物的合成与表征

李宏哲1,2, 刘成有1, 杨景海2, 李雪飞2   

  1. 1. 通化师范学院 物理系, 吉林 通化 134002|2. 吉林师范大学 物理学院, 吉林 四平 136000
  • 收稿日期:2012-08-27 出版日期:2013-05-26 发布日期:2013-05-17
  • 通讯作者: 刘成有 E-mail:cyliu20032003@yahoo.com.cn

Synthesis and Characterization of Graphite\|Carbon Nitride Microbelts

LI Hong zhe1,2, LIU Cheng you1, YANG Jing hai2, LI Xue fei2   

  1. 1. Department of Physics, Tonghua Normal University, Tonghua 134002, Jilin Province, China;
    2. College of Physics, Jilin Normal University, Siping 136000, Jilin Province, China
  • Received:2012-08-27 Online:2013-05-26 Published:2013-05-17
  • Contact: LIU Cheng you E-mail:cyliu20032003@yahoo.com.cn

摘要:

通过高温分解三聚氰胺制备富氮的g-C3N4微米级带状化合物, 并对其纳米带的形貌和结构通过X射线衍射(XRD)、 扫描电子显微镜(SEM)、 化学元素分析(CEA)和X射线光电子能谱(XPS)进行表征. 结果表明: 制备的带状结构规则均一, 带宽约为3~6 μm, 带长为数百微米或几毫米; 样品的石墨相为C3N4结构. 

关键词: 高温分解, 三聚氰胺, 制备, 带状化合物, 石墨相C3N4

Abstract:

Nitrogen\|rich g-C3N4 nanobelts were  synthesized via the pyrolysis of melamine (C3N6H6). The as\|synthesized microbelts are structurally uniform, and each belt is uniform in width and thickness along its length direction. The typical width is in a range of 3 μm to 6  μm. The typical length of the belts is in a range of several hundreds of micrometers, some of which  even have a length of millimeters. The structure and morphology were researched by XRD, SEM, CEA and XPS measurement. The result indicates the sample is graphite-C3N4. 

Key words: pyrolysis, melamine, preparation; , banded compounds, graphite phase C3N4

中图分类号: 

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