Journal of Jilin University Science Edition

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Structure and Bioactivity of Hydroxyapatite Coatings on PureTitanium Fabricated by Microarc Oxidation

YU Weixian1, LIU Xinchan2, WANG Wentian3, ZHANG Yufeng4, WANG Hairui5   

  1. 1. Key Laboratory of Mechanism of Tooth Development and Bone Remodeling and Regeration,School of Stomatology, Jilin University, Changchun 130021, China;2. School of Stomatology, Beihua University, Jilin 132013, Jilin Province, China; 3. Department of Anesthesiology, School of Stomatology, Jilin University, Changchun 130021, China; 4. Department of Prosthodontics, School of Stomatology, Jilin University, Changchun 130021, China;5. School of Materials Science and Engineering, Harbin Institute of Technology, Harbin 150090, China
  • Received:2013-03-26 Online:2014-01-26 Published:2014-03-05
  • Contact: ZHANG Yufeng E-mail:568949871@qq.com

Abstract:

Porous hydroxyapatite(HA)ceramic coating on pure titanium (TA2) substrate was fabricated by microarc oxidation (MAO) in electrolytic solution containing calcium acetate monohydrate and sodium biphosphate dihydrate salt. The morphology, phase and composition of the coating were characterized by scanning electron microscopy (SEM), Xray diffraction (XRD), energy dispersive Xray spectrometry (EDS) and Fourier transmission infrared spectrometry (FT-IR). The bioactivity of the HA ceramic coating was investigated by simulated body fluid (SBF) tests in vitro. The result shows that the ceramic coating was formed on pure titanium substrate, and hydroxyapatite phase was found in the ceramic coating after the microarc oxidation for 10 min. Moreover, HA ceramic coating was proved to be of excellent bioactivity from the carbonatecontaining HA formation on the ceramic coating surfaces. The coatings of MAO are covered completely by the carbonatecontaining HA ceramic coatings after 48 h exposure to simulated body fluid.

Key words: pure titanium, microarc oxidation, ceramic membrane, hydroxyapatite, bioactivity

CLC Number: 

  • TB383