三异丙醇胺硼酸酯的合成与表征

Journal of Jilin University Science Edition

Previous Articles Next Articles

Synthesis and Characterization of Triisopropanolamine Borate

WANG Wei^1, XIU Zhiming^2, WANG Deli^2, XU Tianshu^2,GUO Youming^2, WANG Liping^2

1. Department of Pharmaceutical Engineering, College of Humanities & InformationChangchun University of Techonology, Changchun 130122, China;
2. College of Life Science, Jilin University, Changchun 130012, China

Received:2013-12-06 Online:2014-07-26 Published:2014-09-26
Contact: WANG Liping E-mail:wanglp@jlu.edu.cn

Abstract

Abstract:

Triisopropanolamine borate was synthesized through the esterification of triisopropanolamine and boric acid, and purified by recrystallization. The structure of triisopropanolamine borate was characterized by MS, ¹H NMR and FTIR. Effects of raw material ratio, reaction temperature, reaction time, and reaction solvent on the synthesis, and those of recrystallization solvent and solvent ratio on the purification were investigated. The product was obtained with a purity of 99.8% and a yield of 87.1%, respectively.

Key words: triisopropanolamine borate, synthesis, purification

CLC Number:

O627

WANG Wei, XIU Zhiming, WANG Deli, XU Tianshu,GUO Youming, WANG Liping. Synthesis and Characterization of Triisopropanolamine Borate[J].Journal of Jilin University Science Edition, 2014, 52(04): 831-834.

[1]	LI Erqiang, CHEN Kaijian, ZHOU Yang. Controllable Multi-texture Extended Synthesis and Transfer [J]. Journal of Jilin University Science Edition, 2021, 59(3): 577-586.
[2]	ZHANG Tingyu, CUI Xu, WANG Ying, LI Xuemei, ZHANG Jiayan, ZHUANG Changfu. Synthesis of Ferrocene Porphyrin and Its Substituent Effect [J]. Journal of Jilin University Science Edition, 2021, 59(2): 408-414.
[3]	LIN Hongyan, LI Jiahui, ZENG Ling, WANG Qinglin. Synthesis and Property of AndersonType PolyoxometalateBasedCopper Complex Hybridized by a Tetrazole [J]. Journal of Jilin University Science Edition, 2020, 58(4): 997-1002.
[4]	HUANG Xidai. Fuzzy Region Judgment Algorithm in Network Intrusion [J]. Journal of Jilin University Science Edition, 2020, 58(2): 321-328.
[5]	LIU Rong, WANG Tao, YAO Xin. Selfpropagating Combustion Synthesis and PhotoluminescentProperties of Pure Phase CaAl₄O₇∶Tb³⁺(Sm³⁺)#br# [J]. Journal of Jilin University Science Edition, 2019, 57(1): 166-170.
[6]	LI Qingjie, BAO Haiying, BAU Tolgor, LI Yu. Chemical Composition and Antiinflammatory Activity of Inonotus hispidus#br# [J]. Journal of Jilin University Science Edition, 2019, 57(1): 177-181.
[7]	DONG Xue, XU Yuxin, GUO Jing, GONG Zhongkuo, XIA Linya, YIN Yuhe gmei. Preparation and Identification of Recombinant-Humanized AntiVEGF Monoclonal Antibody [J]. Journal of Jilin University Science Edition, 2019, 57(06): 1538-1543.
[8]	LIN Hongyan, ZHAO Jing, LIU Yu, ZENG Ling, WANG Qinglin. Synthesis, Structure and Dye Adsorption Property of OneDimensional[JP]Flexible Bispyridyltetrazolebased Copper Complex [J]. Journal of Jilin University Science Edition, 2018, 56(4): 1012-1016.
[9]	LI Zheng, YU Miao. Synthesis and Fluorescence Properties of Mesotetra(N-alkyl)-carbazolylporphyrins and Their Lanthanide Acetylacetone Complexes [J]. Journal of Jilin University Science Edition, 2016, 54(06): 1445-1450.
[10]	ZHAO Xia, LI Jia. Polyaniline Nanofibre/Fe₃O₄ Nanoparticle MagneticHybrid for Fast Separation of Pb²⁺ in Water [J]. Journal of Jilin University Science Edition, 2015, 53(05): 1034-1038.
[11]	LIU Hong, ZHANG Shugong. Facial Expression Synthesis Based on Curve Representation [J]. Journal of Jilin University Science Edition, 2015, 53(01): 80-88.
[12]	KONG Weiping, WANG Cong, XU Dandan, ZHAO Li, ZOU Yongcun. High Temperature Hydrothermal Synthesis of PtFunctionalized Mesoporous Al₂O₃ andIts Catalytic Activity for Benzene Combustion [J]. Journal of Jilin University Science Edition, 2014, 52(03): 601-604.
[13]	ZHANG Yaofang, MA Baicheng, TU Peipei, LI Chong, MA Zhihua, JI Yanli,DONG Zhen, MA Chao, HAO Junfeng, LI Xiaodan, WANG Yu, LI Minggang. onstruction and Function Analysis ofDualfunctional Peptide (5rolGLP-HV) [J]. Journal of Jilin University Science Edition, 2014, 52(01): 131-136.
[14]	LIU Hua, WANG Cong, ZOU Xu, LIU Fujian. oft Template Route for Synthesis of Supermicroporous Carbonswith Excellent Adsorption Property for Organic Dye [J]. Journal of Jilin University Science Edition, 2013, 51(06): 1173-1176.
[15]	XIU Zhiming, HUANG Mengyuan, HU Bing, LEI Li\\|yan, WANG Liping. Method Improvement of Synthyesis and Purification of3,4,5,6-Tetrabromophenolsulfonephthalein [J]. Journal of Jilin University Science Edition, 2013, 51(05): 965-968.

Synthesis and Characterization of Triisopropanolamine Borate

PDF (PC)

Like

Knowledge

Abstract

Cite this article

share this article

References

Related Articles 15

Metrics

Comments

Recommended 0