重结晶法制备次氯血红素

J4 ›› 2013, Vol. 51 ›› Issue (02): 330-333.

重结晶法制备次氯血红素

修志明¹, 林琳², 周朋^3, 王丽萍¹

1. 吉林大学生命科学学院, 长春 130012； 2. 北华大学药学院, 吉林吉林 132013；3. 海南大学农学院, 海口 570228

收稿日期:2012-05-29 出版日期:2013-03-26 发布日期:2013-03-27
通讯作者: 王丽萍 E-mail:wanglp@jlu.edu.cn

Preparation of Deuterohemin by Recrystallization Metho

XIU Zhiming¹, LIN Lin², ZHOU Peng³, WANG Liping¹

1. College of Life Science, Jilin University, Changchun 130012, China；2. College of Pharmaceuitcal Science, Beihua University, Jilin 132013, Jilin Province, China；3. College of Agriculture, Hainan University, Haikou 570228, China

Received:2012-05-29 Online:2013-03-26 Published:2013-03-27
Contact: WANG Liping E-mail:wanglp@jlu.edu.cn

摘要/Abstract

摘要：

以氯化血红素为原料, 经间苯二酚还原, 合成了次氯血红素. 采用多次重结晶方法, 使所得的次氯血红素质量分数大于95%, 收率大于85%.

关键词: 血红素；次血红素；重结晶

Abstract:

Deuterohemin was synthesized from hemin via the reduction of resorcinol. By multiple recrystallization, the purification of the heme was resolved. Deuterohemin was obtained, with a purity of more than 95% and a yield of more than 85%.

Key words: hemin, deuterohemin, recrystallization

中图分类号:

Q503

修志明, 林琳, 周朋, 王丽萍. 重结晶法制备次氯血红素[J]. J4, 2013, 51(02): 330-333.

XIU Zhi-Meng, LIN Lin, ZHOU Peng, WANG Li-Ping. Preparation of Deuterohemin by Recrystallization Metho[J]. J4, 2013, 51(02): 330-333.

[1]	陈刚, 尹建元, 王玲, 刘继华. 小鼠血浆中三七皂苷C质量浓度的测定方法[J]. J4, 2010, 48(03): 516-519.
[2]	姜福佳, 王玉萍, 周畅, 张肖建, 周杰, 孟庆繁. 酒糟中蛋白质的提取工艺[J]. J4, 2010, 48(1): 152-156.