急性子总皂苷的提取工艺

J4 ›› 2013, Vol. 51 ›› Issue (03): 522-526.

急性子总皂苷的提取工艺

朱娜^1,2, 孟磊³, 张培旭¹, 姚华¹, 金永日¹, 李绪文¹

1. 吉林大学化学学院, 长春 130012； 2. 吉林省环境监测中心站, 长春 130011；3. 聚光科技股份有限公司, 杭州 310052

收稿日期:2012-08-14 出版日期:2013-05-26 发布日期:2013-05-17
通讯作者: 李绪文 E-mail:xwli@jlu.edu.cn

Extraction of Total Hosenkosides from  Impatiens balsamina L

ZHU Na^1,2, MENG Lei³, ZHANG Peixu¹, YAO Hua¹, JIN Yongri¹, LI Xuwen¹

1. College of Chemistry, Jilin University, Changchun 130012, China|2. Center Station of Supervise Environment of Jilin Province, Changchun 130011, China;3. Focused Photonics Inc., Hangzhou 310052, China

Received:2012-08-14 Online:2013-05-26 Published:2013-05-17
Contact: LI Xuwen E-mail:xwli@jlu.edu.cn

摘要/Abstract

摘要：

考察急性子中4种主要皂苷类化合物凤仙萜四醇苷A,B,C和K, 通过研究乙醇的体积分数、液料比和回流次数等因素对总皂苷提取率的影响, 并设计
正交试验进一步优化, 最终确定急性子总皂苷最优提取条件为： φ(乙醇)=70%, V(液)∶m(料)=6, 回流提取4次, 提取时间分别为60,45,30,30 min. 利用该条件提取急性子总皂苷的提取率为98.19%.

关键词: 急性子, 总皂苷, 正交试验, 提取工艺

Abstract:

Four main hosenkosides, hosenkoside A,B,C and K were used as the indexes of extraction of total hosenkosides from the seeds of Impatiens balsamina L. Solvent concentration, the ratio of material to liquid and reflux time were tested via orthogonal experiments. The confirmed optimum extracting conditions of total hosenkosides were that the seeds of Impatiens balsamina L.were extracted in hot reflux by 70% ethanol V(liquid)∶m(material)=6 for 4 times (60,45,30,30 min, respectively). The results showed that the extraction rate was 98.19%.

Key words: Impatiens balsamina L, total hosenkosides, orthogonal test, extraction process

中图分类号:

R284.2

朱娜, 孟磊, 张培旭, 姚华, 金永日, 李绪文. 急性子总皂苷的提取工艺[J]. J4, 2013, 51(03): 522-526.

SHU Na, MENG Lei, ZHANG Pei-Xu, TAO Hua, JIN Yong-Ri, LI Xu-Wen. Extraction of Total Hosenkosides from  Impatiens balsamina L[J]. J4, 2013, 51(03): 522-526.

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