J4 ›› 2009, Vol. 47 ›› Issue (05): 1065-1070.

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Synthesis of Magnetic Fe3O4 Nanoparticle in Aqueous Phase

WU Jinrui1, XUE Lijuan2, DING Guobin1, HONG Xia3, GUO Yi1,HUANG Yibing1, XU Li1, ZHANG Xuezhong1
   

  1. 1. Key Laboratory for Molecular Enzymology and Engineering of Ministry of Education, Jilin University,Changchun 130021, China|2. First Hospital, |Jilin University, Changchun 130021, China|3. School of Physics, Northeast Normal University, Changchun 130024, China
  • Received:2009-01-16 Online:2009-09-26 Published:2009-11-03
  • Contact: XU Li E-mail:huangyibing@jlu.edu.cn.

Abstract:

In this work, nanometer magnetite (Fe3O4) particles were prepared by the chemical coprecipitation method, NH3·H2O was chosen as the precipitating agent, and was added dropwise together with the mixed aqueous solution containing ferric and ferrousions to the buffer solution composed of NH3·H2O and ammonium nitrate to produce nanometer Fe3O4 particles. Some influence factors on the size and characteristic of the product were investigated, and preliminary characterization was also performed by means of TEM, XRD and IR spectrum.

Key words: chemical coprecipitation, magnetite, nanometer, magnetism

CLC Number: 

  • O648.1