Journal of Jilin University Science Edition

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Preparation and Characterization of Micron Level Spherical CaCO3

LIU Bingshan1, ZOU Haifeng1, GONG Lina1, LV Lei1, ZHENG Keyan1, SHENG Ye1, SHI Ying yan2   

  1. 1. College of Chemistry, Jilin University, Changchun 130012, China;2. Department of Basic Science, Jilin Jianzhu University, Changchun 130118, China
  • Received:2012-10-18 Online:2013-07-26 Published:2013-08-06
  • Contact: SHENG Ye E-mail:shengye@jlu.edu.cn

Abstract:

Spherical calcium carbonate particles were prepared with sodium carboxymethyl cellulose (CMC) as crystalline control agent. Effects of different factors on the morphology and particle size were studied and  optimal synthesis conditions of spherical CaCO3 were obtained. XRD, FTIR, SEM were used to characterize the product. The results indicate that the spherical particles  mainly consisted  of calcite mixed with a small part of vaterite, and the product has good sphericity and uniform particle size in a  range of about 1—3 μm.

Key words: crystalline control agent, sodium carboxymethyl cellulose (CMC), micron spherical particle CaCO3, optimal condition

CLC Number: 

  • O611