J4 ›› 2011, Vol. 49 ›› Issue (04): 767-771.

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AlkaliActivated Synthesis of Zeolite P from Rice Husk

YANG Jun, MA Hongchao, FU Yinghuan, SONG Yu,WANG Yongwei, YU Chunling, DONG Xiaoli   

  1. School of Chemistry Engineering &|Material, Dalian Polytechnic University, Dalian 116034, Liaoning Province, China
  • Received:2010-09-07 Online:2011-07-26 Published:2011-08-16
  • Contact: MA Hongchao E-mail:mhc@sohu.com

Abstract:

Ptype zeolite was synthesized by carbonization, alkalidissolving and hydrothermal method with rice husk and aluminum hydroxide as t
he starting materials without aging prouss and adding crystal seeds. It was found that the optimal zeolitization conditions are temperature 85 ℃; time 8 h; n(Na2O) ∶n(SiO2)=1.43, n(SiO2) ∶n(Al2O3)=4,  n(H2O) ∶n(Na2O)=18.3. The prepared product shows a calcium ionic exchange capacity of 330 mg/g. XRD and SEM of the product show that pure, single phase and high crystalline zeolite P samples were synthesized under optimum conditions.

Key words: rice husk, zeolite P, hydrothermal synthesis, detergent builder

CLC Number: 

  • O613