Nitrogen\|rich g-C3N4 nanobelts were synthesized via the pyrolysis of melamine (C3N6H6). The as\|synthesized microbelts are structurally uniform, and each belt is uniform in width and thickness along its length direction. The typical width is in a range of 3 μm to 6 μm. The typical length of the belts is in a range of several hundreds of micrometers, some of which even have a length of millimeters. The structure and morphology were researched by XRD, SEM, CEA and XPS measurement. The result indicates the sample is graphite-C3N4.