不同基源蜂胶中白杨素和高良姜素含量的比较

J4 ›› 2011, Vol. 37 ›› Issue (4): 675-677.

不同基源蜂胶中白杨素和高良姜素含量的比较

隋殿军¹, 董金香¹, 邱智东¹, 王维¹, 陈雪松², 董雪莲²

1.长春中医药大学|吉林　长春 130117；2.吉林省创智医药开发有限公司|吉林　长春　130051）

收稿日期:2011-03-15 出版日期:2011-07-28 发布日期:2011-07-28
作者简介:隋殿军（1955-）|男|吉林省长春市人|教授|博士生导师|主要从事中医临研究。
基金资助:
技部攻关项目资助课题（2001BA701A07-36）

Comparisonas of |contents of baicalein and galangin in propolis of different origins

SUI Dian-Jun¹, DONG Jin-Xiang¹, QIU Zhi-Dong¹, WANG Wei¹, CHEN Xue-Song², DONG Xue-Lian²

（1.School of Pharmaceutical Sciences,Changchun University ofChinese Medicine,Changchun 130117|China；2.Chuang-zhi Medical Development Company Limited,Jilin Province,Changchun 130051|China）

Received:2011-03-15 Online:2011-07-28 Published:2011-07-28

摘要/Abstract

摘要：

目的：比较13个产地的蜂胶中白杨素和高良姜素的含量。方法：采用高效液相谱法(HPLC)，以十八烷基硅烷键合硅胶为固定相，分别以甲醇-0.15%磷酸（60∶40）和甲醇-0.15%磷酸（65∶35）为流动相；检测波长均为268 nm，检测13个产地的蜂胶中白杨素和高良姜素的含量。结果：在13个产地中均采集5个样本，白杨素和高良姜素含量均超过2.0%和1.8%的为吉林蛟河和河南长葛地区，且前者高于后者（P<0.05），与其他11个产地比较差异均具有统计学意义（P<0.05）。结论：吉林蛟河和河南长葛地区的蜂胶白杨素和高良姜素的含量较高，其品质较优。

关键词: 蜂胶；高效液相色谱法；白杨素；高良姜素

Abstract:

Abstract:Objective
To compare the contents of baicalein and galangin in propolis of different origins.Methods The contents of baicalein and galangin in 13 kinds of prololis of different origins were determinated by high performance liquid chromatography (HPLC).The　samples were separeted by C18 cloumn with the mobile phase of methanol-0.15% phosphoric (60∶40) and methanol-0.15% phosphoric (65∶35),the wavelength of detection was 268 nm.Results Five samples were collected in each area.The contents of baicalein and galangin in propolis of Jilin Jiaohe and Henan Changge were higher,all over　2.0% and 1.8%,and the former was higher than the later(P<0.05);compared with the other 11 areas,there were significant differences（P<0.05）.Conclusion The contents of baicalein and Galangin in propolis of Jilin Jiaohe and Henan Changge are higher.

Key words: propolis；high performance liquid chromatography；baicalein；galangin

中图分类号:

R931

隋殿军, 董金香, 邱智东, 王维, 陈雪松, 董雪莲. 不同基源蜂胶中白杨素和高良姜素含量的比较[J]. J4, 2011, 37(4): 675-677.

SUI Dian-Jun, DONG Jin-Xiang, QIU Zhi-Dong, WANG Wei, CHEN Xue-Song, DONG Xue-Lian. Comparisonas of |contents of baicalein and galangin in propolis of different origins[J]. J4, 2011, 37(4): 675-677.