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Synthesis and Characterization of β-D-Glucopyranosyl Thiourea
SUN Wei-dong, WANG Xiao-ming, ZHANG Suo-qin, LI Yao-xian, ZHENG Ji-fu, YUAN Hong, GUO Qing-huan
J4. 2006, 44 (01):
109-112.
2,3,4,6-Tetra-O-acetyl-β-D-glucopyranosyl thiourea compounds were synthesised from the reaction of aniline and 2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl isothiocyanate in acetonitrile under reflux. The 2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl isothiocyanate was synthesised from 2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl bromine. The structures of the title compounds were confirmed by elemental analyses, IR, MS and 1H NMR spectra.
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