吉林大学学报(工学版) ›› 2014, Vol. 44 ›› Issue (3): 712-717.doi: 10.13229/j.cnki.jdxbgxb201403022

• Orignal Article • Previous Articles     Next Articles

Surface microstructure and properties of 3Cr13 martensitic stainless steel after high current pulsed electron beam bombardment

GUAN Qing-feng,JI Le,CAI Jie,YANG Sheng-zhi,LIU Shi-chao,ZHANG Zai-qiang,HOU Xiu-li   

  1. College of Materials Science and Engineering, Jiangsu University, Zhenjiang 212013, China
  • Received:2013-03-12 Online:2014-03-01 Published:2014-03-01

RICH HTML

0   

PDF (PC)

479

Abstract: The surface of 3Cr13 martensitic stainless steel was irradiated by High Current Pulsed Electron Beam (HCPEB). The microstructures of specimens before and after irradiation were characterized in detail using XRD, SEM and TEM. The mechanical property and corrosion resistance of irradiated samples were examined. It was observed that, after HCPEB irradiation, a melting layer with depth of about 4 μm was formed on the surface. Further microstructural investigations indicate that the surface melted layer consists of nanocrystalline austenite and fine carbide particles, which primarily appear at grain boundary triple junction. The microhardness of the irradiated surface was increased significantly. The electrochemical corrosion resistance of the irradiated surfaces was also improved obviously. The formation of the nanocrystalline austenite layer induced by HCPEB was believed to be the dominating reason for the improvement of comprehensive performance of the material surface.

Key words: metallic materials, high-current pulsed electron beam (HCPEB), 3Cr13 martensitic stainless steel, microstructure, nanocrystalline austenite, corrosion resistance

CLC Number: 

  • TG156.99
[1] Lo K H, Shek C H, Lai J K L. Recent developments in stainless steels[J]. Materials Science and Engineering, 2009, 65(4-6): 39-104.
[2] Akgün O V, rgen M, akir A F. The effect of heat treatment on corrosion behavior of laser surface melted 304L stainless steel[J]. Materials Science and Engineering, 1995, 203(1-2): 324-331.
[3] Kochmanski P, Nowacki J. Activated gas nitriding of 17-4ph stainless steel[J]. Surface and Coatings Technology, 2006, 200(22-23): 6558-6562.
[4] Kang H J, Yoo J S, Park J T, et al. Effect of nano-carbide formation on hydrogen-delayed fracture for quenching and tempering steels during high-frequency induction heat treatment[J]. Materials Science and Engineering, 2012, 543: 6-11.
[5] Proskurovsky D I, Rotshtein V P, Ozur G E, et al. Pulsed electron-beam technology for surface modification of metallic materials[J]. Journal of Vacuum Science & Technology A: Vacuum, Surfaces, and Films,1998,16(4):2480-2488.
[6] 邱冬华,程笃庆,关庆丰,等. 强流脉冲电子束作用下纯镍表面应力特征[J]. 高压物理学报,2009, 23(5):321-326.
Qiu Dong-hua, Cheng Du-qing, Guan Qing-feng, et al. Surface stress characteristics in pure nickel after high current pulsed electron beam irradiation[J]. Chinese Journal of High Pressure Physics, 2009, 23(5):321-326.
[7] Pogrebnjak A D, Bratushka S, Boyko V I, et al. A review of mixing processes in Ta/Fe and Mo/Fe systems treated by high current electron beams[J]. Nuclear Instruments and Methods in Physics Research Section B, 1998, 145(3): 373-390.
[8] 邹慧,关庆丰,张庆瑜,等. 利用强流脉冲电子束对45#钢进行表面改性[J]. 吉林大学学报:工学版, 2004,34(1):127-131.
Zou Hui, Guan Qing-feng, Zhang Qing-yu, et al. Surface modification of 45# steel by high- current pulsed electron beam[J]. Journal of Jilin University(Engineering and Technology Edition), 2004,34(1):127-131.
[9] 赵乃勤. 合金固态相变[M]. 长沙:中南大学出版社, 2008:101-106.
[10] Guan Q F, Zou H, Zou G T, et al. Surface nanostructure and amorphous state of a low carbon steel induced by high-current pulsed electron beam[J]. Surface & Coating Technology, 2005, 196(1-3):145-149.
[11] Tang Guan-ze,Xu Fang-jun,Fan Guo-hua,et al.Mechanisms of microstructure formations in M50 steel melted layer by high current pulsed electron beam[J]. Nuclear Instruments and Methods in Physics Research Section B:Beam Interactions with Materials and Atoms, 2012,288:1-5.
[12] 关庆丰,邹阳,张在强. 强流脉冲电子束作用下纯铜的微观结构和腐蚀性能[J]. 吉林大学学报:工学版, 2013,43(4):964-969.
Guan Qing-feng, Zou Yang, Zhang Zai-qiang. Microstructures and corrosion property of pure copper under high current pulsed electron beam irradiation[J]. Journal of Jilin University(Engineering and Technology Edition), 2013, 43(4):964-969.
[13] Zhang K M, Yang D Z, Zou J X, et al. Improved in vitro corrosion resistance of a NiTi alloy by high current pulsed electron beam treatment[J]. Surface & Coatings Technology, 2006, 201(6): 3096-3102.
[1] JIANG Qiu-yue,YANG Hai-feng,TAN Cai-wang. Strengthening properties of welded joints of 22MnB5 super high strength steel [J]. Journal of Jilin University(Engineering and Technology Edition), 2018, 48(6): 1806-1810.
[2] ZHENG Xiao-yi, SUN Da-qian, LI Xin, DU Gui-gang, XIN Wei-da, REN Zhen-an. Microstructure and properties of cladded Al-Nb layers reinforced by NbAl3 [J]. Journal of Jilin University(Engineering and Technology Edition), 2018, 48(5): 1531-1536.
[3] GUAN Qing-feng, DONG Shu-heng, ZHENG Huan-huan, LI Chen, ZHANG Cong-lin, LV-Peng. Cr surface alloying of 45# steel by high-current pulsed electron beam treatment [J]. 吉林大学学报(工学版), 2018, 48(4): 1161-1168.
[4] ZHAO Yu-guang, YANG Xue-hui, XU Xiao-feng, ZHANG Yang-yang, NING Yu-heng. Effects of Al-10Sr modifiers with different states, modification temperature and holding time on microstructure of ZL114A alloy [J]. 吉林大学学报(工学版), 2018, 48(1): 212-220.
[5] ZHANG Zhi-qiang, LIU Cong-hao, HE Dong-ye, LI Xiang-ji, LI Ji-xuan. Effect of hot stamping process of boron steel on shape precision based on performance gradient distribution [J]. 吉林大学学报(工学版), 2017, 47(6): 1829-1833.
[6] TANG Hua-guo, MA Xian-feng, ZHAO Wei, LIU Jian-wei, ZHAO Zhen-ye. Synthesis microstructure and thermal properties of high performance bulk Al [J]. 吉林大学学报(工学版), 2017, 47(5): 1542-1547.
[7] GUAN Qing-feng, ZHANG Yuan-wang, SUN Xiao, ZHANG Chao-ren, LYU Peng, ZHANG Cong-lin. Surface alloying of Al-W alloy by high current pulsed electron beam treatment [J]. 吉林大学学报(工学版), 2017, 47(4): 1171-1178.
[8] CUI Ya-nan, HAN Ji-wei, FENG Lei, LI Jia-di, WANG Le. Microstructure of asphalt under salt freezing cycles [J]. 吉林大学学报(工学版), 2017, 47(2): 452-458.
[9] LIU Xiao-bo, ZHOU De-kun, ZHAO Yu-guang. Microstructure and mechanical property of Mg2Si/Al composites fabricated by semi-solid extrusion under different isothermal heat treatments [J]. 吉林大学学报(工学版), 2016, 46(5): 1577-1582.
[10] YANG Yue, ZHOU Lei-lei. Effect of micro-arc oxidation treatment on corrosion resistance of aluminum friction stir welding welds [J]. 吉林大学学报(工学版), 2016, 46(2): 511-515.
[11] LI Chun-ling, FAN Ding, WANG Bin, YU Shu-rong. 5A06 aluminum alloy and galvanized steel butt welding-brazing by laser with preset filler powder [J]. 吉林大学学报(工学版), 2016, 46(2): 516-521.
[12] ZHANG Jia-tao, ZHAO Yu-guang, TAN Juan. Effect of starting microstructure on refining potency of electro-pulsing on reverse austenite grain [J]. 吉林大学学报(工学版), 2016, 46(1): 193-198.
[13] GUAN Qing-feng, LI Yan, HOU Xiu-li, YANG Sheng-zhi, WANG Xiao-tong. Modification of solid solution Mg-Gd-Y-Nd alloy irradiated by high current pulsed electron beam [J]. 吉林大学学报(工学版), 2015, 45(4): 1200-1205.
[14] MA Yun-hai, SHANG Wen-bo, FAN Xue-ying, GAO Zhi-hui, TONG Jin, YAN Zhi-feng, CHANG Zhi-yong. Preparation and degradation of porous β-tricalcium phosphate bioceramic for bone imitaion [J]. 吉林大学学报(工学版), 2015, 45(4): 1367-1374.
[15] GAO Song, LIANG Ji-cai, CHEN Guang-yi, WEI Zhi-yong, TENG Fei. Rapid adjusting of fundamental units in process of flexible 3D stretch-bending [J]. 吉林大学学报(工学版), 2014, 44(6): 1723-1728.
Viewed
Full text


Abstract

Cited
  Shared   
  Discussed   
[1] LIU Song-shan, WANG Qing-nian, WANG Wei-hua, LIN Xin. Influence of inertial mass on damping and amplitude-frequency characteristic of regenerative suspension[J]. 吉林大学学报(工学版), 2013, 43(03): 557 -563 .
[2] CHU Liang, WANG Yan-bo, QI Fu-wei, ZHANG Yong-sheng. Control method of inlet valves for brake pressure fine regulation[J]. 吉林大学学报(工学版), 2013, 43(03): 564 -570 .
[3] LI Jing, WANG Zi-han, YU Chun-xian, HAN Zuo-yue, SUN Bo-hua. Design of control system to follow vehicle state with HIL test beach[J]. 吉林大学学报(工学版), 2013, 43(03): 577 -583 .
[4] ZHU Jian-feng, LIN Yi, CHEN Xiao-kai, SHI Guo-biao. Structural topology optimization based design of automotive transmission housing structure[J]. 吉林大学学报(工学版), 2013, 43(03): 584 -589 .
[5] HU Xing-jun, LI Teng-fei, WANG Jing-yu, YANG Bo, GUO Peng, LIAO Lei. Numerical simulation of the influence of rear-end panels on the wake flow field of a heavy-duty truck[J]. 吉林大学学报(工学版), 2013, 43(03): 595 -601 .
[6] WANG Tong-jian, CHEN Jin-shi, ZHAO Feng, ZHAO Qing-bo, LIU Xin-hui, YUAN Hua-shan. Mechanical-hydraulic co-simulation and experiment of full hydraulic steering systems[J]. 吉林大学学报(工学版), 2013, 43(03): 607 -612 .
[7] ZHANG Chun-qin, JIANG Gui-yan, WU Zheng-yan. Factors influencing motor vehicle travel departure time choice behavior[J]. 吉林大学学报(工学版), 2013, 43(03): 626 -632 .
[8] MA Wan-jing, XIE Han-zhou. Integrated control of main-signal and pre-signal on approach of intersection with double stop line[J]. 吉林大学学报(工学版), 2013, 43(03): 633 -639 .
[9] YU De-xin, TONG Qian, YANG Zhao-sheng, GAO Peng. Forecast model of emergency traffic evacuation time under major disaster[J]. 吉林大学学报(工学版), 2013, 43(03): 654 -658 .
[10] XIAO Yun, LEI Jun-qing, ZHANG Kun, LI Zhong-san. Fatigue stiffness degradation of prestressed concrete beam under multilevel amplitude cycle loading[J]. 吉林大学学报(工学版), 2013, 43(03): 665 -670 .
Copyright © Journal of Jilin University(Engineering and Technology Edition), All Rights Reserved.
Tel: +86-431-85095297　Fax: +86-431-85094074　E-mail: xbgxb@jlu.edu.cn
Powered by Beijing Magtech Co. Ltd