胶粉改性沥青老化机理及表征评价研究综述

doi:10.13229/j.cnki.jdxbgxb.20230651

吉林大学学报(工学版) ›› 2024, Vol. 54 ›› Issue (1): 22-43.doi: 10.13229/j.cnki.jdxbgxb.20230651

胶粉改性沥青老化机理及表征评价研究综述

唐乃膨^1,²(),薛晨阳²,刘少鹏³,朱洪洲^1,²(),李睿^1,²

^1.重庆交通大学交通土建工程材料国家地方联合工程研究中心，重庆 400074
^2.重庆交通大学土木工程学院，重庆 400074
^3.交通运输部规划研究院，北京 100028

收稿日期:2023-04-13 出版日期:2024-01-30 发布日期:2024-03-28
通讯作者: 朱洪洲 E-mail:tnp@cqjtu.edu.cn;zhuhongzhouchina@cqjtu.edu.cn
作者简介:唐乃膨（1990-），男，副教授，博士.研究方向：路面材料及结构.E-mail：tnp@cqjtu.edu.cn
基金资助:
国家自然科学基金项目(51808073);重庆市教育委员会科学技术研究计划青年项目(KJQN202100725);重庆市自然科学基金项目(cstc2021jcyj-msxmX0637);重庆市研究生联合培养基地建设项目(JDLHPYJD2020014);重庆市研究生科研创新项目(CYS23482)

Review on aging mechanism， characterization and evaluation of crumb rubber modified asphalt

Nai-peng TANG^1,²(),Chen-yang XUE²,Shao-peng LIU³,Hong-zhou ZHU^1,²(),Rui LI^1,²

^1.National ＆ Local Joint Engineering Research Center for Transportation Civil Engineering Materials，Chongqing Jiaotong University，Chongqing 400074，China
^2.School of Civil Engineering，Chongqing Jiaotong University，Chongqing 400074，China
^3.Transport Planning and Research Institute，Ministry of Transport，Beijing 100028，China

Received:2023-04-13 Online:2024-01-30 Published:2024-03-28
Contact: Hong-zhou ZHU E-mail:tnp@cqjtu.edu.cn;zhuhongzhouchina@cqjtu.edu.cn

摘要/Abstract

摘要：

综述了国内外对胶粉改性沥青老化机理、表征及评价的研究现状。胶粉改性沥青的老化过程伴随着胶粉的溶胀、降解反应以及沥青与胶粉之间的物质交互作用；胶粉改性沥青老化行为的表征主要从化学组分、分子结构、分子量、表面形貌入手，并解释其对宏观性能的影响；胶粉改性沥青老化性能评价主要采用黏度、复数模量、低温蠕变劲度、疲劳寿命等流变学指标，且通常与微观表征及化学方法相结合。然而，当前国内外对胶粉改性沥青老化过程中填料迁移行为关注较少，特别是炭黑、白炭黑等填料的作用机理有待进一步挖掘；缺乏胶粉改性沥青多组分老化特征同步表征方法；缺乏统一的老化评价指标，且大多研究在混合料老化性能验证方面存在不足。最后，提出了胶粉改性沥青老化机理及表征评价研究的发展趋势与展望。

关键词: 道路工程, 胶粉改性沥青, 综述, 老化机理, 老化表征, 老化评价

Abstract:

State of the art of the aging mechanism， characterization and evaluation of CRMA at home and abroad are summarized. The aging process of CRMA is accompanied by swelling， degradation reaction of crumb rubber and the interaction between asphalt and crumb rubber. The aging behavior of CRMA is mainly characterized from the chemical components， molecular structure， molecular weight and surface morphology， and their effects on macroscopic properties are explained. Rheological parameters such as viscosity， complex shear modulus， creep stiffness at low temperature and fatigue life are mainly used to evaluate the aging performance of CRMA， which are usually combined with microscopic characterization and chemical methods. However， during the aging process of CRMA， the migration behavior of fillers， e.g.， carbon black， white carbon black， received less attention. In addition， there is a lack of simultaneous characterization method for multi-component aging characteristics of CRMA. There are no universal aging evaluation indexes for CRMA， and most of the studies are insufficient in the aging performance verification at mixture level. The development trend and prospect of aging mechanism， characterization and evaluation of CRMA are proposed.

Key words: road engineering, crumb rubber modified asphalt, review, aging mechanism, aging characterization, aging evaluation

中图分类号:

U414

唐乃膨,薛晨阳,刘少鹏,朱洪洲,李睿. 胶粉改性沥青老化机理及表征评价研究综述[J]. 吉林大学学报(工学版), 2024, 54(1): 22-43.

Nai-peng TANG,Chen-yang XUE,Shao-peng LIU,Hong-zhou ZHU,Rui LI. Review on aging mechanism， characterization and evaluation of crumb rubber modified asphalt[J]. Journal of Jilin University(Engineering and Technology Edition), 2024, 54(1): 22-43.

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不同沥青		老化机理	老化机理异同				总结
不同沥青		老化机理	沥青氧化	聚合物降解	溶胀作用	物质交互	总结
基质沥青		老化过程中发生吸氧氧化反应，轻质组分挥发，生成含氧官能团，沥青中大分子增多^［32］。	发生	无	无	无	胶粉改性沥青老化机理与基质沥青和SBS改性沥青不同，更加复杂。
SBS改性沥青		沥青氧化老化及SBS聚合物的老化共同发生，两者相互作用，减轻老化进度^{［33，34］}。	发生	发生	短期老化存在溶胀与再交联现象	发生
胶粉改性沥青	橡胶沥青	老化过程中发生沥青的氧化^［35］、胶粉溶胀^［36］、降解^［37］及胶粉中炭黑等填料的迁移^［38］。胶粉的溶胀、降解及填料迁移能够改善沥青的抗老化性能，延缓老化进程。	发生	短期老化较弱，长期老化剧烈	短期老化剧烈，长期老化较弱	发生
	脱硫胶粉改性沥青		发生	与胶粉初始脱硫降解程度相关	与胶粉初始脱硫降解程度相关	发生
	TB胶粉改性沥青		发生	整个老化过程都较弱	整个老化过程都较弱	发生

老化机理	机理简述	研究现状	局限性
胶粉溶胀作用	胶粉吸收沥青轻质组分而发生溶胀，同时在颗粒表面形成沥青质含量很高的凝胶膜^［39］	研究较多，但多集中于胶粉改性沥青的短期老化	对溶胀作用的研究多集中于短期老化，缺乏对长期老化过程中溶胀作用的系统研究；胶粉和沥青的物质交互作用研究较少，缺乏明确的结论
胶粉脱硫降解	橡胶网状大分子结构适度氧化解聚，变成大量的小体型网状结构和少量链状物^［38］	研究较为成熟，结论明确
沥青氧化老化	沥青老化过程中，轻质组分受热与氧气发生反应，生成硬质组分，并产生新的官能团^［57］	研究较多，且研究结论较为明确
物质交互作用	沥青老化过程中，胶粉发生解聚，炭黑、白炭黑等填料进入到沥青相中，对沥青相产生影响^［38］	研究较少，且缺乏明确的研究结论

老化时间/d	饱和分/%	芳香分/%	胶质/%	沥青质/%
0	16.53	32.09	40.52	10.86
2	15.39	30.24	41.01	13.36
4	15.05	28.47	37.72	18.76
6	14.14	26.82	35.59	23.45
8	14.38	24.43	30.52	30.67
10	13.96	21.26	28.57	36.21

老化表征	试验方法	研究现状	局限性
化学组分变化	SARA ^［65］、对SARA的改进^［9］、TLC-FID ^［67］、GC-MS ^［70］	表征方法较多，研究结论成熟	各类表征方法之间关联较弱，缺乏对胶粉改性沥青老化过程中微观层面变化的同步表征方法；缺乏基于相态分离的有效表征方法；且一些表征方法在应用于胶粉改性沥青时仍存在不足，需要创新
分子结构变化	FTIR ^［76］、NMR ^［81］、TG ^［82］、DSC ^［83］	表征方法较多，结论明确
分子量变化	GPC ^［89］	研究结果较为明确，但方法单一，且在胶粉改性沥青表征中存在不足
微观形貌变化	SEM ^［99］、AFM ^［103］	表征方法较多，结论明确
基于相态分离的变化	胶粉筛析分离实验及溶剂洗脱实验^［107］、显微试验与FTIR试验的结合^［108］	研究较少，且当前表征方法存在一定的缺陷

老化指标	基质沥青^{［129?135］}	SBS改性沥青^{［34，136?138］}	胶粉改性沥青^{［102，114，115，122，123，139］}	总结
常规指标	针入度、软化点、延度			目前对于胶粉改性沥青老化的评价与常规沥青区别不明显，都是以流变学指标为主；结合微观结构特征评价沥青的老化状态
高温流变指标	车辙因子、黏度、复模量、相位角
高温流变指标	不可恢复蠕变柔量、恢复率
低温流变指标	劲度模量、蠕变速率等
疲劳指标	疲劳因子	疲劳寿命
微观指标	官能团指标、微观形貌、四组分变化、分子量
粘附性指标	应用较少	接触角、表面自由能	应用较少

胶粉改性沥青老化机理及表征评价研究综述

Review on aging mechanism， characterization and evaluation of crumb rubber modified asphalt

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老化评价	老化指标	研究现状	局限性
基于高温性能	PAR、ISP、DAR、VAI、\|G\|、δ、R、J_nr、 \|G\|/sinδ等^{［102，113-116］}	各种性能指标种类较多，能够根据不同性能需求展开胶粉改性沥青的老化性能评价	各类指标评价标准不统一，流变学指标与微观指标之间的关联性较差，缺乏具有代表性的胶粉改性沥青老化状态评价指标体系
基于低温性能	m、S、S/m、C_T、k值、S_A等^{［78，117，118］}
基于疲劳性能	N_f、\|G\|sinδ、CAI等^{［117，119，120］}
高低温及疲劳性能结合	相对影响因子^［121］
基于流变学与微观结合的老化评价	流变学指标结合FTIR指标^{［122-124］}	研究较多，存在较多流变学与微观结合的评价指标与老化模型
	流变学指标结合组分分析^{［27，125］}
	流变学指标结合微观形貌^［126］
	流变学指标结合各类微观指标^{［102，127］}

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