Heat resistant bulk Al was prepared by mechanical milling, cold isostatic pressing and press-forming technique. The bulk Al possesses stable microstructure, with grain size between 0.6 and 4 μm, and the ultimate tensile strength, 536 MPa, surpasses that of most commercial Al alloys, especially at high temperature. The heat exposure experiment was carried out at 200 ℃, 300 ℃ and 350 ℃ for 4320 h. The high temperature endurance strength is 381 MPa, 242 MPa and 178 MPa corresponding to 200 ℃, 300 ℃ and 350 ℃ respectively. The pinning action of the second-phase dispersoids in bulk Al highly restrains grain growth during the process of hating.